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The solid-state transformations upon heating of cis-[Ir-(CO)2Cl(C5H5N)] have been studied by combining complementary techniques which allowed some light to be shed on a complex solid-state process. It was found that during quick heating polycrystalline cis-[Ir(CO)2Cl(C5H5N)] experiences an anisotropic thermal expansion of the lattice along the Ir-Ir chain, followed by a fast, irreversible rearrangement at about 73 C into a phase of higher symmetry which subsequently undergoes at about 74 C a reversible solid-solid phase transition and becomes amorphous. If the compound is immediately and properly cooled, a partial recrystallization takes place, accompanied by significant microstructural changes.

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    1 0 年前
    最佳解答

    The solid-state transformations upon heating of cis-[Ir-(CO)2Cl(C5H5N)] have been studied by combining complementary techniques which allowed some light to be shed on a complex solid-state process.

    固體變革在熱化同邊[Ir- (CO) 2Cl (C5H5N)] 通過結合在一個複雜固體過程允許一些光是棚子的補全技術學習了。

    It was found that during quick heating polycrystalline cis-[Ir(CO)2Cl(C5H5N)] experiences an anisotropic thermal expansion of the lattice along the Ir-Ir chain, followed by a fast, irreversible rearrangement at about 73 C into a phase of higher symmetry which subsequently undergoes at about 74 C a reversible solid-solid phase transition and becomes amorphous.

    它被發現在快的熱化多晶同邊期間[Ir (CO) 2Cl (C5H5N)] 體驗格子的非均質性的熱擴散沿Ir-Ir鏈子,由快速跟隨, 不可逆的重新整理在大約73C到隨後接受在大約74C反演性solid-solid相變并且變得無定形的階段更高的對稱裡。

    If the compound is immediately and properly cooled, a partial recrystallization takes place, accompanied by significant microstructural changes.

    如果立刻和適當地冷卻化合物, 部份再結晶發生, 由重大的微結構變動陪同。

    參考資料: 自己
  • 1 0 年前

    固體變革在熱化同邊[Ir (CO)2Cl(C5H5N) ] 由結合學習了允許一些光是棚子在一個複雜固體過程的補全技術。它被發現在快的熱化多晶同邊[Ir(CO)2Cl(C5H5N) 期間] 體驗格子的非均質性的熱擴散沿Ir Ir 鏈子, 被快速, 不可逆的重新整理隨後了而來在大約73?C 入接受在大約74?C 反演性solid-solid 階段轉折和隨後變得無定形的階段更高的對稱。如果化合物立刻和適當地冷卻, 部份再結晶發生, 由重大的微結構變動陪同。

    參考資料: 網路
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